Thermomechanical Analysis (TMA)

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TMA measurement of multilayer film thickness by a penetration test. Layer thickness is annotated on the plot

Thermomechanical analysis (TMA) probes the response of the sample’s thermal, dynamic, and static-mechanical properties as the ambient temperature around a sample is changed over time.

See also: Dynamic Mechanical Analysis (DMA), which can be performed under variable temperature conditions e to achieve similar results to TMA experiments.

Strengths

Limitations

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Sample Requirements

TMA Example Outputs

TMA measurement of dimensional change (shrinkage and expansion) of oriented polyethylene film acquired in tensile mode.

TMA measurement of multilayer film thickness by a penetration test. Layer thickness is annotated on the plot

TMA Instruments Used

Anton Paar MCR 702

Anton Paar MCR 702

The MCR 702 MultiDrive is a combination DMA / Rheometer with the flexibility and precision to facilitate a huge array of test mode options.

  • Maximum Torque: 230 mNm
  • Normal Force Range: 0.005 N to 50 N
  • Maximum Temperature: 1000 °C
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During a TMA measurement, a probe is set at rest on the surface of a sample with no applied force. Then, heat is applied, causing the temperature to rise and inducing material property changes that deform the specimen.

Hyper-fine measurements are taken of the probe’s vertical displacement, illuminating the sample’s morphological and mechanical response to temperature flux.

During heating, one can also apply a controlled force across the probe (either dynamic/variable or unchanging/static), enabling different measurement modes that assess a wide assortment of mechanical properties as a function of temperature.

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