Battery Tear-down

Full battery tear-down with materials and component characterization

Access the Heart of the Battery

To optimize your batteries, you’ve got to understand the effects of variations in your raw materials, processing conditions, cell formation, cycling, aging, and environmental conditions. Covalent’s full-service battery tear-down can reveal how all these factors inform your battery’s operating lifespan and performance.

Careful separation of all components for subsequent testing. Samples are handled continuously in an air-free environment to safeguard against any degradation or environmental effects.

Covalent’s metrology experts will use battery-specific testing methods to provide comprehensive insight into the chemical and material characteristics of your battery components.

Typical Turnaround Time: 2 Weeks for Full Service

What to Expect

  • Complete Component Separation: Individual components (anode, cathode, separator, and electrolyte) will be isolated and carefully prepared for chemical analysis and morphological characterization.
    • Optionally, any gas in the cell can also be collected for analysis.
  • All Handling Under Protective Atmosphere: to avoid any incidental environmental impacts or component degradation due to oxygen (or other gas) exposure, all samples are handled under a protective, inert atmosphere.
  • Expert Visual Inspection: Experts will analyze the cell and components to identify any anomalies (particles, defects, etc.). Any and all findings will be captured in a report with photographic documentation.
  • Full Report: Receive full documentation of the tear-down process and procedures, all key findings, observations, and conclusions.

Your comprehensive report will provide:

  • Executive Summary that will highlight the most important results and insights relevant to your project goals.
  • Detailed findings, graphs, and images from each component investigated.
  • Expert recommendations and observations guiding your next investigative steps and / or improvements to the system.
  • Images of the cell before tear-down (via X-ray Imaging or Micro-CT).
  • FULL RAW DATA is available for each characterization technique requested.

Covalent accepts batteries in any cell format with any chemistry. They may be fresh or cycled, though their state of charge (SOC) must be fully discharged.

Get Complete Insight into Your Batteries

Chemistry

Morphology

Structure

Anode
Chemistry

Elemental: SEM-EDS Mapping (top-down, x-section)

Organics: FTIR, Pyrolysis GC-MS, TGA for binder analysis

Surface: XPS, x-section with TEM

Morphology
  • Broad-beam Ion Mill Cross-sectioning
  • Top-down and X-section SEM Imaging
Structure
  • Optical Microscopy
  • Visual Inspection of components
  • Foil dimensions
  • Active material mass loading

Cathode
Chemistry

Elemental: SEM-EDS Mapping (top-down, x-section), Stoichiometry by ICP-OES

Organics: FTIR, Pyrolysis GC-MS, TGA for binder analysis

Lithium Plating: ToF-SIMS

Morphology
  • Broad-beam Ion Mill Cross-sectioning
  • Top-down and X-section SEM Imaging
Structure
  • Optical Microscopy
  • Visual Inspection of components
  • Foil dimensions
  • Active material mass loading

Separator
Chemistry

Elemental: SEM-EDS Mapping (top-down, x-section)

Polymer: FTIR

Coating: FTIR

Morphology
  • Broad-beam Ion Mill Cross-sectioning
  • Top-down and X-section SEM Imaging
  • Porometry
Structure
  • Optical Microscopy
  • Visual Inspection of components

Electrolyte
Chemistry

Organics: GCMS

Salts: Liquid NMR (1H, 13C, 19F, 31P)

Salts & Contaminants: ICP-MS


Gas (Optional)
Chemistry

Organics: GCMS


Electrochemical Characterization of Components

Half Cell Construction

Covalent experts will select electrodes made from standard components in accordance with materials harvested and the use case of interest for your measurements.

The half-cells are assembled once again in an air-free environment in a coin-cell format.

Instruments Used

Cycling and EIS are performed with Maccor Cyclers and Gamry Potentiostats.

Covalent’s Analytical Techniques for Battery Characterization

TechniquePowdersSlurriesElectrodes & FoilsSeparatorsElectrolyte (liquid/solid)Full Battery & Failure Analysis
Visual Inspection
X-ray / CT
SAM
Optical Microscopy
SEM-EDS
TEM-EDS + EELS
AFM
XPS / SIMS
Auger
XRF
GDOES
ICP-MS / ICP-OES
GCMS
NMR
FTIR
Raman
XRD
TGA / DSC
DMA
Rheology
Nanoindentation
PSA
DLS / Zeta
BET
Porometry
Porosimetry
Pycnometry
Wettability
Electrochemical Testing

Ready to Get Started?

Click below to contact Covalent’s Experts about your Battery testing needs.
We can’t wait to work with you!